Indentation + User defined profile Max load : 1000.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 20.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 1000.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 20.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 1000.00 mN Loading rate : 6000.00 mN/min Pause : 60.0 s Max load : 0.00 mN Loading rate : 6000.00 mN/min Date : 13-05-06 Time : 09:46:38 Method : Oliver & Pharr Cycle n? 1 + Main results Hv= 3.5285 Vickers H= 34.615 MPa E= 1.6187 GPa + Hypothesis Poisson= 0.30 + Additional results Pm= 1002.72 mN Hm= 11461.91 nm S= 0.3390 mN/nm Hc= 9307.47 nm Ht= 8504.06 nm H0= 5882.01 nm m= 1.95 Epsilon= 0.73 Ac= 28968124416.00 nm? Cycle n? 2 + Main results Hv= 3.5151 Vickers H= 34.483 MPa E= 1.6526 GPa + Hypothesis Poisson= 0.30 + Additional results Pm= 1002.82 mN Hm= 11457.78 nm S= 0.3467 mN/nm Hc= 9344.12 nm Ht= 8565.47 nm H0= 6208.52 nm m= 1.87 Epsilon= 0.73 Ac= 29081122816.00 nm? Cycle n? 3 + Main results Hv= 3.5135 Vickers H= 34.467 MPa E= 1.6693 GPa + Hypothesis Poisson= 0.30 + Additional results Pm= 1003.07 mN Hm= 11447.10 nm S= 0.3503 mN/nm Hc= 9350.88 nm Ht= 8583.91 nm H0= 6362.01 nm m= 1.83 Epsilon= 0.73 Ac= 29101969408.00 nm? Measured values Time (s) Pd (nm) Fn (mN) 0 0 0 0 0 0.3617 27.7176 0.9582 0 0 0.7233 60.4503 1.9731 0 0 1.085 86.159 2.9672 0 0 1.4467 99.9382 4.0815 0 0 1.8084 581.4382 38.2995 0 0 2.17 969.3322 68.7669 0 0 2.5317 1388.7893 108.8579 0 0 2.8934 1685.2137 138.5118 0 0 3.255 2080.0308 178.7325 0 0 3.6167 2481.8892 218.8891 0 0 3.9784 2775.6833 248.4453 0 0 4.3401 3163.7756 288.9086 0 0 4.7017 3449.2368 318.7914 0 0 5.0634 3829.4111 358.5436 0 0 5.4251 4187.1553 398.9794 0 0 5.7868 4456.584 428.6898 0 0 6.1484 4813.5518 468.7869 0 0 6.5101 5176.7041 509.0136 0 0 6.8718 5449.0376 538.8339 0 0 7.2334 5802.1689 579.0271 0 0 7.5951 6068.1289 608.8077 0 0 7.9568 6434.4351 648.575 0 0 8.3185 6804.9468 688.7789 0 0 8.6801 7074.9375 718.8372 0 0 9.0418 7454.9355 758.7603 0 0 9.4035 7730.5776 788.5714 0 0 9.7651 8099.1016 828.8347 0 0 10.1268 8463.5781 868.8631 0 0 10.4885 8737.6973 898.9107 0 0 10.8502 9091.167 938.8293 0 0 11.2118 9356.3037 969.0257 0 0 11.5735 9698.6699 1005.652 0 0 11.9352 9860.4033 1003.1542 0 0 12.2968 9954.2529 1003.3679 0 0 12.6585 10045.5 1003.3373 0 0 13.0202 10128.0273 1003.0825 0 0 13.3819 10177.4355 1003.1893 0 0 13.7435 10235.6934 1003.2305 0 0 14.1052 10277.1523 1003.2778 0 0 14.4669 10320.8223 1003.1375 0 0 14.8286 10368.3711 1003.3206 0 0 15.1902 10398.915 1003.5189 0 0 15.5519 10428.9648 1002.8872 0 0 15.9136 10455.1123 1003.2225 0 0 16.2752 10486.9688 1003.3571 0 0 16.6369 10514.166 1003.4152 0 0 16.9986 10538.3623 1003.319 0 0 17.3603 10559.918 1003.554 0 0 17.7219 10579.1895 1003.191 0 0 18.0836 10605.458 1003.2855 0 0 18.4453 10632.3682 1003.2198 0 0 18.8069 10647.0947 1002.9741 0 0 19.1686 10663.2471 1003.049 0 0 19.5303 10685.9189 1003.0504 0 0 19.892 10704.0146 1003.261 0 0 20.2536 10723.2959 1003.4594 0 0 20.6153 10734.4795 1003.0628 0 0 20.977 10753.502 1003.4915 0 0 21.3386 10760.5703 1003.1267 0 0 21.7003 10774.4238 1003.1069 0 0 22.062 10794.8584 1003.2824 0 0 22.4237 10811.1074 1003.4245 0 0 22.7853 10823.209 1003.0504 0 0 23.147 10839.0234 1003.1267 0 0 23.5087 10850.541 1003.4991 0 0 23.8704 10865.0791 1003.2534 0 0 24.232 10871.0049 1003.4487 0 0 24.5937 10883.7266 1003.5082 0 0 24.9554 10898.2793 1002.9086 0 0 25.317 10910.6533 1003.5546 0 0 25.6787 10916.9453 1003.2183 0 0 26.0404 10923.9014 1003.4075 0 0 26.4021 10936.8779 1003.5021 0 0 26.7637 10942.5352 1003.5143 0 0 27.1254 10955.752 1003.0268 0 0 27.4871 10967.8115 1003.2427 0 0 27.8487 10977.8047 1003.1695 0 0 28.2104 10983.5859 1003.3282 0 0 28.5721 10990.9814 1003.348 0 0 28.9338 10995.3721 1003.2032 0 0 29.2954 11006.1699 1003.2503 0 0 29.6571 11021.668 1003.3251 0 0 30.0188 11020.2031 1002.8803 0 0 30.3804 11030.4941 1003.3236 0 0 30.7421 11040.0693 1003.3145 0 0 31.1038 11051.8711 1003.0642 0 0 31.4655 11053.9736 1003.2732 0 0 31.8271 11060.957 1003.3326 0 0 32.1888 11071.3848 1003.0154 0 0 32.5505 11077.4053 1003.4884 0 0 32.9122 11080.5566 1003.2554 0 0 33.2738 11087.0791 1003.2321 0 0 33.6355 11090.9375 1003.1199 0 0 33.9972 11104.6064 1003.1558 0 0 34.3588 11110.6309 1003.1924 0 0 34.7205 11114.3447 1003.1325 0 0 35.0822 11118.8281 1003.3663 0 0 35.4439 11124.5244 1003.1806 0 0 35.8055 11130.4688 1003.2763 0 0 36.1672 11134.1689 1003.1085 0 0 36.5289 11133.8213 1003.3892 0 0 36.8905 11143.1729 1003.3846 0 0 37.2522 11154.2363 1003.4533 0 0 37.6139 11162.7617 1002.9348 0 0 37.9756 11164.2773 1003.3206 0 0 38.3372 11166.9697 1003.1536 0 0 38.6989 11170.3164 1002.8841 0 0 39.0606 11181.1719 1003.2656 0 0 39.4222 11185.1445 1003.2166 0 0 39.7839 11189.0664 1003.3236 0 0 40.1456 11193.8779 1003.2296 0 0 40.5073 11193.9043 1003.1771 0 0 40.8689 11206.8086 1003.4868 0 0 41.2306 11205.252 1003.1442 0 0 41.5923 11216.4453 1003.5296 0 0 41.9539 11216.6514 1003.2955 0 0 42.3156 11217.5039 1003.1245 0 0 42.6773 11225.2529 1003.1451 0 0 43.039 11231.5156 1003.6049 0 0 43.4006 11229.2109 1003.264 0 0 43.7623 11240.6123 1003.9202 0 0 44.124 11247.1182 1003.1277 0 0 44.4857 11249.0205 1003.2824 0 0 44.8473 11248.5557 1003.5052 0 0 45.209 11258.1982 1002.8857 0 0 45.5707 11265.5508 1003.406 0 0 45.9323 11265.499 1003.3403 0 0 46.294 11267.4971 1003.374 0 0 46.6557 11272.6104 1003.0358 0 0 47.0174 11275.9736 1003.3411 0 0 47.379 11278.9316 1003.1008 0 0 47.7407 11282.541 1003.2974 0 0 48.1024 11283.3369 1003.2946 0 0 48.464 11286.8076 1003.3861 0 0 48.8257 11290.9746 1003.3206 0 0 49.1874 11297.0635 1003.5433 0 0 49.5491 11300.2188 1003.2195 0 0 49.9107 11302.2295 1003.1801 0 0 50.2724 11309.9053 1003.235 0 0 50.6341 11312.0391 1003.3907 0 0 50.9958 11317.8037 1003.0093 0 0 51.3574 11316.4736 1003.1656 0 0 51.7191 11318.0166 1002.9852 0 0 52.0808 11324.7305 1003.1909 0 0 52.4424 11324.2627 1003.1055 0 0 52.8041 11323.4385 1003.142 0 0 53.1658 11332.3643 1003.2369 0 0 53.5275 11332.6465 1003.3994 0 0 53.8891 11344.7314 1003.1954 0 0 54.2508 11340.5176 1003.3382 0 0 54.6125 11344.3594 1003.3756 0 0 54.9741 11344.0146 1003.1085 0 0 55.3358 11350.2109 1003.2332 0 0 55.6975 11350.8691 1003.3145 0 0 56.0592 11354.2217 1003.0618 0 0 56.4208 11357.8906 1003.4205 0 0 56.7825 11363.6387 1003.3037 0 0 57.1442 11370.6543 1003.1702 0 0 57.5058 11371.0449 1003.4304 0 0 57.8675 11367.1221 1003.1509 0 0 58.2292 11372.9873 1003.1609 0 0 58.5909 11379.7471 1003.1801 0 0 58.9525 11379.9092 1003.1696 0 0 59.3142 11380.4961 1003.2583 0 0 59.6759 11388.7441 1003.2478 0 0 60.0376 11385.7676 1003.1262 0 0 60.3992 11391.3955 1003.4121 0 0 60.7609 11392.0576 1003.1971 0 0 61.1226 11399.2568 1003.1022 0 0 61.4842 11403.3721 1003.3206 0 0 61.8459 11404.1631 1003.2786 0 0 62.2076 11403.6563 1003.2778 0 0 62.5693 11408.6963 1003.4634 0 0 62.9309 11408.6611 1002.7948 0 0 63.2926 11409.3018 1003.2183 0 0 63.6543 11414.7168 1003.3508 0 0 64.0159 11416.2998 1003.0877 0 0 64.3776 11416.8613 1003.1085 0 0 64.7393 11420.2129 1003.4807 0 0 65.101 11424.8398 1003.2397 0 0 65.4626 11427.1436 1002.8801 0 0 65.8243 11429.4697 1003.4897 0 0 66.186 11434.7705 1002.8272 0 0 66.5476 11428.8174 1003.1299 0 0 66.9093 11434.084 1003.3327 0 0 67.271 11434.2744 1003.0138 0 0 67.6327 11438.1836 1003.3457 0 0 67.9943 11436.0518 1003.3571 0 0 68.356 11443.5947 1003.1942 0 0 68.7177 11442.9365 1003.2868 0 0 69.0794 11446.877 1003.2623 0 0 69.441 11452.833 1003.156 0 0 69.8027 11451.3467 1003.3434 0 0 70.1644 11451.3789 1003.2161 0 0 70.526 11455.5313 1003.0968 0 0 70.8877 11454.8467 1003.3719 0 0 71.2494 11459.6816 1003.0607 0 0 71.6111 11461.9072 1002.7209 0 0 71.9727 11406.4453 966.956 0 0 72.3344 11316.4902 927.6943 0 0 72.6961 11216.6709 889.9066 0 0 73.0577 11123.2637 855.1594 0 0 73.4194 11029.0879 818.7087 0 0 73.7811 10919.2061 782.5787 0 0 74.1428 10807.707 746.2936 0 0 74.5044 10678.6904 709.2547 0 0 74.8661 10560.5156 674.0583 0 0 75.2278 10437.9883 637.7259 0 0 75.5894 10298.1318 601.7457 0 0 75.9511 10151.3711 565.1477 0 0 76.3128 10001.5957 529.0124 0 0 76.6745 9848.6094 492.8922 0 0 77.0361 9674.8613 456.7424 0 0 77.3978 9486.9297 420.5023 0 0 77.7595 9293.9199 384.35 0 0 78.1211 9081.8799 348.3654 0 0 78.4828 8850.2988 312.0985 0 0 78.8445 8601.4268 275.908 0 0 79.2062 8336.6211 239.0734 0 0 79.5678 8057.4268 203.5278 0 0 79.9295 7755.6646 167.3941 0 0 80.2912 7421.1587 131.2941 0 0 80.6529 7053.7695 95.3115 0 0 81.0145 6640.6108 58.5621 0 0 81.3762 6118.8931 23.0304 0 0 81.7379 5572.3193 2.7773 0 0 82.0995 5410.21 3.5738 0 0 82.4612 5283.1641 3.5151 0 0 82.8229 5185.833 3.6927 0 0 83.1846 5119.0249 3.4941 0 0 83.5462 5056.5142 3.5026 0 0 83.9079 4997.7271 3.7102 0 0 84.2696 4954.0073 3.4708 0 0 84.6312 4915.1479 3.5961 0 0 84.9929 4872.52 3.5863 0 0 85.3546 4841.0894 3.6735 0 0 85.7163 4803.5322 3.3724 0 0 86.0779 4777.1294 3.3649 0 0 86.4396 4756.3208 3.7237 0 0 86.8013 4728.1509 3.304 0 0 87.1629 4703.2148 3.5662 0 0 87.5246 4682.5938 3.4933 0 0 87.8863 4663.3579 3.3883 0 0 88.248 4644.6865 3.6157 0 0 88.6096 4629.3032 3.575 0 0 88.9713 4613.2632 3.2833 0 0 89.333 4594.5415 3.5214 0 0 89.6947 4579.1797 3.5734 0 0 90.0563 4559.625 3.3987 0 0 90.418 4543.9214 3.2552 0 0 90.7797 45...
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